Microwave-assisted Allylic Oxidation at C-13 Position of 14-Deoxysinenxan A

Microwave-assisted allylic oxidation at C-13 position of 14-deoxysinenxan A wasdescribed. This new method (150℃/10 mir/5 bar on microwave synthesizer) led to a better yieldof compound 1 and shorter reaction time.

作 者： Jun GU Meng ZHANG Da Li YIN Ji Yu GUO Xiao Tian LIANG   作者單位： Institute of Materia Medica, Chinese Academy of Medical Sciences & Peking Union Medical College, Beijing 100050  刊 名： 中國化學(xué)快報（英文版）  ISTIC SCI 英文刊名： CHINESE CHEMICAL LETTERS  年，卷(期)： 2005 16(4)  分類號：   關(guān)鍵詞： Allylic oxidation   microwave   14-deoxysinenxan A  

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